INTERCALATED COMPOUNDS OF GRAPHITE OXIDE WITH FLUORINE-SUBSTITUTED DERIVATIVES OF DODECAHYDRO-CLOSO-DODECABORIC ACID AND ITS SALTS AND METHOD OF OBTAINING SAID COMPOUNDS Russian patent published in 2009 - IPC C01B31/04 C01B35/00 

FIELD: chemistry.

SUBSTANCE: invention can be used in making solid electrolytes. Intercalated compounds of graphite oxide with fluorine-substituted derivatives of dodecahydro-closo-dodecaboric acid and its salts with composition C₄O_xH_y×nR_zB₁₂H_12-mF_m, where x=0.58-1.98, y=0.54-0.75, 0.4≤n≤1.98, z=2 for R - H⁺, NH₄ ⁺, Li⁺, Na⁺, K⁺ or z=1 for R - Zn²⁺, Mg²⁺, Ca²⁺, Sr²⁺, Ba²⁺; m=2, 4 to 8, 10, 12 are obtained through combined concentration of aqueous gel of graphite oxide with fluorine-substituted derivatives of dodecahydro-closo-dodecaboric acid and its salts, taken in molar ratio 1:(0.4 to 1.98). The mixture is constantly stirred at temperature not above 40°C until formation of a solid product with subsequent drying over a dehydrating agent to constant weight.

EFFECT: obtaining compounds with high ion conduction.

3 cl, 2 tbl, 19 ex