METHOD OF PROCESSING REACTION MIXTURE FORMED DURING NUCLEOPHILIC SYNTHESIS OF POLYARYLENE ETHER KETONES Russian patent published in 2009 - IPC C08G65/40 

Abstract RU 2373230 C2

FIELD: chemistry.

SUBSTANCE: method is proposed for processing a reaction mixture formed during synthesis of polyarylene ether ketones by reacting an aromatic dihalogen compound with bisphenol and/or halogen phenol in the presence of a carbonate of alkali and/or alkali-earth metals in a high-boiling aprotic solvent to form a polyarylene ether ketone, which involves steps for crushing the solidified reaction mixture in the presence of water, two-step washing with organic solvent and water and drying the washed product, wherein during two-stage washing, wet crushed reaction mixture has residual moisture of 1 to 30 wt %.

EFFECT: reduced residual content of salts and reaction solvent without hardware overhead.

3 cl, 6 ex

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RU 2 373 230 C2

Authors

Rikhter Aleksander

Shimann Vera

Gjuntsel' Bernd

Jilg Boris

Ulikh Vil'Frid

Dates

2009-11-20Published

2007-05-11Filed