FIELD: chemistry.
SUBSTANCE: method is proposed for processing a reaction mixture formed during synthesis of polyarylene ether ketones by reacting an aromatic dihalogen compound with bisphenol and/or halogen phenol in the presence of a carbonate of alkali and/or alkali-earth metals in a high-boiling aprotic solvent to form a polyarylene ether ketone, which involves steps for crushing the solidified reaction mixture in the presence of water, two-step washing with organic solvent and water and drying the washed product, wherein during two-stage washing, wet crushed reaction mixture has residual moisture of 1 to 30 wt %.
EFFECT: reduced residual content of salts and reaction solvent without hardware overhead.
3 cl, 6 ex
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Authors
Dates
2009-11-20—Published
2007-05-11—Filed