FIELD: chemistry.
SUBSTANCE: invention relates to making ceramic material for mecidine, which can be used in traumatology and orthopaedics, maxillofacial surgery, as well as a drug carrier. A method is proposed for making ceramic biodegradable material consisting of calcium pyrophosphate and tricalcium phosphate, involving preparation of a mixture consisting of calcium pyrophosphate and hydroxyapatite in mass ratio of these components in the interval 75/25-5/95, moulding and roasting. Pyrophosphate is obtained through thermal treatment of brushite powder CaHPO4*2H2O, synthesised from aqueous solutions of calcium nitrate and ammonium hydrophosphate with concentration of 1M-2M, at 550-650°C for 10-20 minutes. When roasting, the ceramics are held at an intermediate temperature range of 700-800°C in isothermic conditions for 1.5-2.5 hours.
EFFECT: obtaining biodegradable material with a uniform microstructure and controlled rate of resorption.
3 cl, 1 ex, 1 tbl
| Title | Year | Author | Number | 
|---|---|---|---|
| METHOD FOR MAKING BIODEGRADABLE CERAMIC COMPOSITE OF DOUBLE POTASSIUM CALCIUM PHOSPHATE | 2008 | 
 | RU2395303C1 | 
| METHOD FOR PREPARING SUBMICRON BIPHASIC TRICALCIUM PHOSPHATE AND HYDROXYAPATITE CERAMICS | 2013 | 
 | RU2555685C2 | 
| METHOD OF PREPARING MIXTURE FOR PRODUCING CERAMIC BIODEGRADABLE MATERIAL | 2010 | 
 | RU2456253C2 | 
| METHOD FOR PREPARING CALCIUM PYROPHOSPHATE POROUS CERAMICS | 2012 | 
 | RU2531377C2 | 
| METHOD OF OBTAINING POROUS CALCIUM PYROPHOSPHATE | 2012 | 
 | RU2537615C2 | 
| METHOD OF PREPARING CALCIUM PYROPHOSPHATE POWDER CAPABLE OF AGGLOMERATION | 2008 | 
 | RU2395450C1 | 
| CALCIUM PYROPHOSPHATE-BASED CERAMIC BIODEGRADABLE MATERIAL MANUFACTURE METHOD | 2008 | 
 | RU2392006C2 | 
| METHOD FOR MAKING CERAMIC BIODEGRADABLE MATERIAL BASED ON CALCIUM AND SODIUM PHOSPHATES | 2007 | 
 | RU2372891C2 | 
| METHOD OF PRODUCING HYDROXYAPATITE BASED CERAMIC, CONTAINING ZINC OXIDE | 2007 | 
 | RU2372313C2 | 
| MANUFACTURE METHOD OF CALCIUM PHOSPHATE-BASED POROUS MATERIAL | 2008 | 
 | RU2392007C2 | 
Authors
Dates
2010-06-10—Published
2008-12-30—Filed