FIELD: chemistry.
SUBSTANCE: present invention relates to a method of producing N-trimethylsilylamido-chloroanhydride of methyl-phosphonic acid of formula CH3P(O)(Cl)NHSi(CH3)3 and can be used in organic synthesis. The disclosed method of producing N-trimethylsilylamido-chloroanhydride of methyl-phosphonic acid involves reacting dichloroanhydride of methyl-phosphonic acid with hexamethyldisilazane at 60-70°C for 4-6 hours without a solvent.
EFFECT: obtaining a new reagent for organic synthesis.
1 cl, 2 ex
Authors
Dates
2010-07-20—Published
2008-12-15—Filed