METHOD OF PRODUCING TRIMETHYLALKOXYSILANES Russian patent published in 2024 - IPC C07F7/04 C07F7/18 

Abstract RU 2814974 C1

FIELD: chemistry.

SUBSTANCE: invention relates to methods of producing trimethylalkoxysilanes. Disclosed is a method of producing trimethylalkoxysilanes by reacting the corresponding alcohol with hexamethyldisilazane in ratio (alcohol : hexamethyldisilazane) = 2:1.05 without using a solvent with addition of 0.4–1.0% moles of methylphosphonic acid as a catalyst. For separation and purification of target substances obtained using this method, it is not required to use a method of azeotropic rectification, fractionation is sufficient.

EFFECT: reduced staging, cheapening of production processes and increased output of trimethylalkoxysilanes of high purity for synthesis of physiologically active substances.

5 cl, 3 tbl, 5 ex

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RU 2 814 974 C1

Authors

Kapashin Valerij Petrovich

Mandych Vladimir Grigorevich

Isaev Ilya Nikolaevich

Veriga Valerij Lvovich

Ilyasov Ildar Khamzeevich

Vetkin Danil Olegovich

Isaeva Anna Yurevna

Kopylov Aleksandr Anatolevich

Dates

2024-03-07Published

2023-06-19Filed