METHOD OF OBTAINING PURE DECAPHENYL CYCLOPENTASILANE Russian patent published in 2010 - IPC C07F7/07 

Abstract RU 2400485 C1

FIELD: chemistry.

SUBSTANCE: invention discloses a method of obtaining pure decaphenyl cyclopentasilane by reacting freshly distilled diphenyl dichlorosilane with ultra-fine lithium metal in a medium of dry tetrahydrofuran, taken in ratio of 1:2 at temperature between minus 10°C and minus 20°C and then treatment of the reaction mass with distilled water.

EFFECT: design of a method of obtaining decaphenyl cyclopentasilane, which ensures high output and low cost of the desired product while maintaining high purity of the desired product.

1 cl, 3 ex

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Authors

Storozhenko Pavel Arkad'Evich

Sheludjakov Viktor Dmitrievich

Lebedev Anatolij Viktorovich

Lebedeva Alla Borisovna

Ustinova Ol'Ga Leonidovna

Shatunov Valerij Vladimirovich

Kozyrkin Boris Ivanovich

Orlov Vitalij Jur'Evich

Dates

2010-09-27Published

2009-05-07Filed