METHOD FOR PREPARING BLOOD SAMPLE FOR GAS CHROMATOGRAPHY OF ORGANOCHLORINE PESTICIDES Russian patent published in 2011 - IPC G01N33/50 G01N33/48 G01N33/00 G01N1/10 G01N30/02 

Abstract RU 2414711 C2

FIELD: medicine.

SUBSTANCE: for an assay, 5-7 cm3 of blood is taken, and before extraction the sample is pre-treated with 2 cm3 of 60% sulphuric acid; the extraction process is executed with 30 cm3 of n-hexane once, and gas chromatography is preceded with single treatment of n-hexane extract with 10 cm3 of concentrated sulphuric acid.

EFFECT: invention provides higher reliability of α-HCCH, γ-HCCH test results and twofold reduced time of sample preparation.

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RU 2 414 711 C2

Authors

Sof'Ina Lidija Ivanovna

Zarja Natal'Ja Jur'Evna

Tekutskaja Elena Evgen'Evna

Gusaruk Ljubov' Ramazanovna

Dates

2011-03-20Published

2008-12-26Filed