FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing 2-methyl-1,4-naphthoquinone (menadione, vitamin K3) which is widely used as a preparation for improving blood clotting. The method involves oxidation of 2-methylnaphthalene-containing material with hexavalent chromium compounds in an acidic medium. The 2-methylnaphthalene-containing material used is a methylnaphthalene fraction sampled in temperature interval 235-245°C with distillation of stillage bottoms formed when producing naphthalene from the naphthalene fraction of coal tar.
EFFECT: invention enables to obtain an end product using a simple and highly efficient method with higher utilisation of starting material.
2 cl, 3 ex
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Authors
Dates
2011-06-10—Published
2009-12-07—Filed