FIELD: chemistry.
SUBSTANCE: invention can be used for photocatalytic treatment of water and air from organic compounds and pathogenic flora, with photocatalytic decomposition of water. In order to obtain a photocatalytic nanocomposite containing titanium dioxide, a transition metal salt is added in amount of 1.5-60 wt % in terms of metal to a titanium (IV) salt solution with concentration of 1.0-2.5 mol/l TiO2 while stirring and the salts undergo hydrolysis in ammonium hydroxide solution at 15-25°C for 0.1-0.25 hours with formation of a precipitate. The obtained precipitate is settled for 1.5-2.0 hours, separated, washed and thermally processed at 80-800°C for 0.5-1.0 hours. The titanium (IV) salt used is a chloride or sulphate, the iron (III) salt used is a chloride, sulphate or nitrate, the niobium (V) salt used is a fluoride and the tungsten (VI) salt used is sodium tungstate.
EFFECT: invention enables to increase photocatalytic activity of the titanium dioxide-based nanocomposite in the visible light region, lowers hydrolysis temperature and shortens duration of the method.
9 cl, 1 tbl
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METHOD OF OBTAINING TITANIUM-SILICON SODIUM-CONTAINING COMPOSITION | 2013 |
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RU2575026C1 |
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RU2394926C1 |
METHOD FOR OBTAINING SODIUM-CONTAINING TITANIUM SILICATE | 2014 |
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RU2568699C1 |
METHOD OF PRODUCING TITANIUM DIOXIDE | 2011 |
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RU2472707C1 |
METHOD OF PREPARING TITANIUM OXIDE PHOTOCATALYST ACTIVE IN VISIBLE SPECTRUM | 2012 |
|
RU2520100C1 |
HYBRID CARRIER-SYSTEMS | 2008 |
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RU2491311C2 |
Authors
Dates
2011-12-10—Published
2010-07-20—Filed