METHOD OF PRODUCING 2,6-DIISOBORNYL-4-HYDROXY-4-METHYL-2,5-CYCLOHEXADIEN-1-ONE Russian patent published in 2012 - IPC C07C13/23 

Abstract RU 2458901 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing 2,6-diisobornyl-4-hydroxy-4-methyl-2,5-cyclohexadien-1-one. The method involves oxidation of phenol in an organic solvent by bubbling an oxidant into a reaction mixture or adding an oxidant solution by drops in an organic solvent at temperature from -10 to 40°C. The oxidant used is chlorine dioxide, the phenol used is terpenic phenol, specifically 2,6-diisobornyl-4-methylphenol in an organic solvent. The molar ratio of reactants is equal to 1:1-5, respectively.

EFFECT: invention increases output of 2,6-diisobornyl-4-hydroxy-4-methyl-2,5-cyclohexadien-1-one.

10 cl, 15 ex

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RU 2 458 901 C1

Authors

Loginova Irina Valerianovna

Chukicheva Irina Jur'Evna

Kuchin Aleksandr Vasil'Evich

Dates

2012-08-20Published

2011-03-14Filed