FIELD: chemistry.
SUBSTANCE: described is a method of determining methylphenols in aqueous media, involving chemical modification thereof into acetates, extraction concentration and gas-chromatographic detection, where at the first chemical modification step, the modifier reactant used is iodine in amount of 0.005-0.015% in the presence of ammonium acetate and ammonia in amount of 0.3-1.0% of the weight of the water sample; acylation is carried out in a medium of an organic solvent, and an electron capture detector is used for detection.
EFFECT: high sensitivity of analysis.
7 ex, 2 tbl, 3 dwg
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF DETERMINING CHLORINE-SUBSTITUTED PHENOLS IN AQUEOUS MEDIA | 2011 |
|
RU2475737C1 |
| METHOD OF DETECTING MONONITROPHENOLS IN AQUEOUS MEDIA | 2009 |
|
RU2407000C2 |
| METHOD OF DETECTING CHLOROANILINES IN AQUEOUS MEDIA | 2010 |
|
RU2458343C2 |
| METHOD OF DETECTING HUMIC ACIDS IN AQUEOUS MEDIA | 2009 |
|
RU2402761C2 |
| METHOD OF AQUEOUS MEDIUM ANALYSIS FOR PHENOL CONTENT | 2007 |
|
RU2344417C1 |
| METHOD OF DETECTING ANILINE IN AQUEOUS MEDIA | 2007 |
|
RU2346274C1 |
| METHOD OF DETERMINING PHENOL IN SOIL | 2000 |
|
RU2170926C1 |
| METHOD OF DETERMINING MONOCHLOROPHENOLS IN AQUEOUS MEDIA | 1999 |
|
RU2142627C1 |
| METHOD IDENTIFYING PHENOLS IN AQUEOUS MEDIA | 2000 |
|
RU2183832C2 |
| METHOD OF QUANTITATIVE DETERMINATION OF HEXACHLOROBENZENE IN BLOOD BY METHOD OF GAS CHROMATOGRAPHIC ANALYSIS | 2016 |
|
RU2613306C1 |
