METHOD OF OBTAINING AZIRIDINO[2',3':1,2] FULLERENE[60] Russian patent published in 2012 - IPC C07D203/26 

Abstract RU 2466990 C2

FIELD: chemistry.

SUBSTANCE: invention relates to method of obtaining aziridino[2',3':1,2]fullerene[60] of general formula (1): by interaction of fullerene C60 with hydrazoic acid (HN2), generated in situ by reaction of NaN3 with H2SO4, taken in mole ratio C60:NaN3 : H2SO4=1 : (100-120):(100-120), in chlorobenzene at temperature 60°C for 2-4 hours. Target product is obtained with 24-35% output in one stage.

EFFECT: increase of output of suitable.

1 dwg, 1 tbl

Similar patents RU2466990C2

Title Year Author Number
METHOD OF PRODUCING TRIAZOLINO[4',5':1,2]FULLERENE[60] 2010
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Akhmetov Arslan Rifkhatovich
  • Jarullin Il'Dar Rafisovich
RU2455290C1
METHOD OF PRODUCING AZIRIDINO[2',3':1,9]FULLERENES[60], CONTAINING FRAMEWORK AND POLYCYCLIC SUBSTITUTES 2014
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Akhmetov Arslan Rifkhatovich
  • Khuzin Artur Albertovich
RU2596876C2
METHOD OF PRODUCING 1-BROMO-2-AZIDO-1,2-DIHYDRO(C-I)[5,6]FULLERENE 2013
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Akhmetov Arslan Rifkhatovich
  • Jarullin Il'Dar Rafisovich
RU2551279C2
METHOD FOR PRODUCING N-ARYLAZIRIDINUM[2 ', 3 ': 1.9]FULLERENE [60] 2014
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Akhmetov Arslan Rifkhatovich
  • Ryabinina Tatyana Egorovna
RU2594562C2
METHOD OF OBTAINING POLYHYDRO[60]FULLERENES 2007
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Akhmetov Arslan Rifkhatovich
  • D'Jakonov Vladimir Anatol'Evich
  • Ibragimov Askhat Gabdrakhmanovich
RU2348602C1
METHOD OF PRODUCING 3'-METHYL-3'-FURYL- OR 3'-METHYL-3'-THIENYL-3'H-CYCLOPROPA[1,9](C-I)[5,6]FULLERENES 2011
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Khuzin Artur Al'Bertovich
RU2478629C2
METHOD OF PRODUCING 1-IODO-2-AZIDO(C-I)[5,6]FULLERENE 2011
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Akhmetov Arslan Rifkhatovich
  • Jarullin Il'Dar Rafisovich
  • Gabidullina Linara Akhmedovna
RU2484010C2
METHOD FOR SELECTIVE PRODUCTION OF FULLERENE QUADRICYCLAN DERIVATIVES 2017
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Akhmetov Arslan Rifkhatovich
  • Shakirova Zulfiya Rasimovna
RU2703529C2
METHOD OF SELECTIVE RECEPTION OF ISOPROPYLINE 5'-ARYL-1'N-PYRROLIDINO[3',4':1,9](C60-IH)[5,6]FULLERENE-2'-CARBOXYLATES 2016
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Shakirova Zulfiya Rasimovna
RU2629752C1
METHOD FOR SELECTIVE PRODUCTION OF NORBORNADIENE FULLERENE DERIVATIVES 2017
  • Dzhemilev Usein Memetovich
  • Tuktarov Ajrat Ramilevich
  • Akhmetov Arslan Rifkhatovich
  • Shakirova Zulfiya Rasimovna
RU2703528C2

RU 2 466 990 C2

Authors

Dzhemilev Usein Memetovich

Tuktarov Ajrat Ramilevich

Akhmetov Arslan Rifkhatovich

Jarullin Il'Dar Rafisovich

Dates

2012-11-20Published

2010-12-07Filed