METHOD OF INSERTING QUANTUM DOTS INTO POROUS CALCIUM CARBONATE PARTICLES BY CODEPOSITION Russian patent published in 2014 - IPC C01F11/18 C09K11/00 B01J13/22 B82B3/00 B82Y5/00 B82Y30/00 B82Y40/00 

Abstract RU 2509057 C2

FIELD: chemistry.

SUBSTANCE: porous calcium carbonate particles are formed from the reaction CaCl2+2NaHCO3→CaCO3↓+2NaCl+2H+, wherein an aqueous solution of quantum dots, modified with an excess amount of mercaptoacetic having concentration of 0.05-4 mg/ml, is added to 0.3 M NaHCO3 solution while stirring intensely. The obtained suspension which contains porous calcium carbonate particles with inserted quantum dots is washed 1-3 times with water and once with ethanol, while treating with ultrasound after each washing. The obtained particles are then coated with polyethyleneimine or 6 layers of water-soluble polyelectrolytes from a series which includes diethylaminoethyl-dextran, chitosan, carrageenan.

EFFECT: shorter time for producing porous calcium carbonate particles with 100% inserted quantum dots.

2 cl, 6 ex

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RU 2 509 057 C2

Authors

Sukhanova Tat'Jana Vladimirovna

Sizova Svetlana Viktorovna

Manokhina Veronika Vladimirovna

Shchapov Aleksandr Fedorovich

Olejnikov Vladimir Aleksandrovich

Nabiev Igor' Rufailovich

Dates

2014-03-10Published

2012-03-22Filed