METHOD OF OBTAINING LITHIUM TETRAFLUOROBORATE Russian patent published in 2014 - IPC C01B35/06 C01D15/00 

Abstract RU 2519194 C2

FIELD: chemistry.

SUBSTANCE: invention can be used in chemical industry. Method of obtaining lithium tetrafluoroborate includes addition of lithium borohydrate in tetrahydrofuran into liquid hydrogen fluoride at temperature (-57)-(-53)°C. Solvent is removed in vacuum at temperature 100-105°C. Reaction mass is kept at said temperature for 4 hours with residual pressure 0.03 mm Hg.

EFFECT: invention makes it possible to increase output of target product and its purity.

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RU 2 519 194 C2

Authors

Makarov Grigorij Mikhajlovich

Khotinen Aleksandr Vladimirovich

Voronin Evgenij Konstantinovich

Akhtjamov Oskar Zufarovich

Shchelyvanov Evgenij Jur'Evich

Voronin Aleksandr Evgen'Evich

Dates

2014-06-10Published

2012-07-11Filed