FIELD: chemistry.
SUBSTANCE: sublimation apparatus for fine purification of substances has a heat-insulated heated cover, a heated housing, a sublimation chamber, a desublimation chamber divided into cells by parallel partition walls, arranged with spacing relative to the cover, a heat carrier chamber, a raw material inlet pipe, a process gas outlet pipe, heat carrier inlet and outlet pipes. The housing heater is made of self-contained blocks lying in each cell of the housing. The heat carrier chamber is made of sections, each lying in a cell. The heat carrier inlet pipes have a check valve. A self-contained block is a high-frequency generator.
EFFECT: providing a repeated sublimation-desublimation process without using manual labour, low power consumption, shorter time for maintenance of the sublimation apparatus and unit cost of the purified product, high specific output.
2 cl, 4 dwg
Title | Year | Author | Number |
---|---|---|---|
DESUBLIMATION APPARATUS | 2012 |
|
RU2487742C1 |
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SUBLIMATION APPARATUS | 0 |
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SU1517974A1 |
METHOD OF PURIFYING ZIRCONIUM FROM HAFNIUM | 2010 |
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DESUBLIMATOR | 2011 |
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DESUBLIMATION DEVICE | 2007 |
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DESUBLIMATOR | 2011 |
|
RU2467780C1 |
SUBLIMATION STILL | 0 |
|
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STATIONARY CONDENSER-EVAPORATOR | 2009 |
|
RU2394624C1 |
STATIONARY CONDENSER-EVAPORATOR | 2007 |
|
RU2339423C1 |
Authors
Dates
2014-08-10—Published
2013-05-06—Filed