FIELD: electricity.
SUBSTANCE: method for manufacturing of nanosized powders for Li4Ti5 O 12/C lithium titanate-based compound includes mixing of titanium dioxide, lithium carbonate and starch and thermal treatment of the obtained mix until material is received with 100% spinel structure. Lithium carbonate is taken in 10÷15 wt % excess from stoichiometrically-defined quantity required for receipt of Li4Ti5 O 12 compound. Starch is introduced in quantity of 10÷20 wt % of the mixture weight. The mixture is treated thermally at temperature of 850°C during 10-15 hours.
EFFECT: invention allows reduced duration of nanopowder synthetic process with receipt of material having grain size of 60-70 nm and high values of discharge capacity.
1 tbl, 1 ex
| Title | Year | Author | Number | 
|---|---|---|---|
| PRODUCTION OF LITHIUM TITANATE NANO-SIZED POWDER | 2013 | 
 | RU2528839C1 | 
| LiCrTiO-BASED MATERIAL OF ANODE IN LITHIUM-ION BATTERY BASED ON SPINEL-STRUCTURE AND METHOD OF ITS PRODUCTION | 2014 | 
 | RU2558140C1 | 
| ANODE MATERIAL FOR LITHIUM ELECTROLYTIC CELL AND METHOD OF PREPARING SAID MATERIAL | 2009 | 
 | RU2397576C1 | 
| COMPOSITE CATHODIC MATERIAL OF LITHIUM ION BATTERY BASED ON LIV(PO)WITH NASIKON STRUCTURE AND METHOD OF ITS OBTAINING | 2013 | 
 | RU2542721C1 | 
| METHOD OF PRODUCING LITHIUM TITANATE | 2009 | 
 | RU2519840C2 | 
| METHOD FOR OBTAINING POWDER OF LITHIUM COBALT OXIDE WITH ALLOYED STRUCTURE AND MODIFIED SURFACE | 2020 | 
 | RU2755526C1 | 
| LITHIUM ACCUMULATOR ANODE ACTIVE MASS MANUFACTURING METHOD | 2017 | 
 | RU2658305C1 | 
| METHOD FOR PRODUCING COMPOSITE ANODE MATERIAL TiNbO/C FOR LITHIUM-ION BATTERIES | 2022 | 
 | RU2799067C1 | 
| METHOD TO PRODUCE HIGHLY DISPERSED CATHODE MATERIALS LiFeMPO/C WITH OLIVINE STRUCTURE | 2010 | 
 | RU2444815C1 | 
| METHOD OF OBTAINING LITHIUM TITANATE WITH SPINEL STRUCTURE | 2013 | 
 | RU2542273C1 | 
Authors
Dates
2015-01-10—Published
2013-07-17—Filed