FIELD: chemistry.
SUBSTANCE: method includes crystallising perfluorodecalin in two steps: at the first step, crystallisation is carried out while reducing the temperature to minus 17°C - minus 18°C at a rate of 1-2°C per minute while stirring; the mass is held at a temperature of minus 17°C - minus 18°C for 30-35 minutes, filtered and dried and the obtained crystals are separated; the crystals are then melted at ambient temperature; at the second step crystallisation is repeated at the same conditions, but while reducing temperature to minus 15°C. The product obtained using the present method has purity higher than 99 wt %.
EFFECT: high purity of the finished product.
6 ex
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Authors
Dates
2015-03-20—Published
2014-01-09—Filed