FIELD: chemistry.
SUBSTANCE: beryllium concentrate is activated by its milling until X-ray amorphous product with size of particles less than 5 mcm is obtained, and bertrandite-phenacite-fluorite concentrate is activated by addition in it of fluorine-containing compounds in quantity which ensures fluorine content 10÷25 wt %. Then, activated beryllium concentrate is processed with sulphuric acid and obtained acid pulp is added to activated bertrandite-phenacite-fluorite concentrate. After that, formed reaction mass is sulphatised for 1.5÷2 h at temperature 115÷125°C with continuous mechanical removal of reaction products from the surface of particles of activated concentrates with the following exposure at temperature 250÷300°C for not less than 1 h.
EFFECT: increase of beryllium extraction in rough beryllium hydroxide due to sedimentation completeness.
2 tbl, 1 ex
Title | Year | Author | Number |
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|
RU2546945C1 |
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|
RU2324653C2 |
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|
RU2351539C2 |
METHOD OF PROCESSING OF BERTRANDITE-PHENACITE-FLUORITE CONCENTRATES | 2006 |
|
RU2325326C2 |
METHOD OF PICKLING RAW MATERIAL OF BERYL JEWELRY BY METHOD OF SELECTIVE CHEMICAL PICKLING | 2017 |
|
RU2661134C1 |
MIXTURE FOR PRODUCING BERYLLIUM SULPHATE FROM MIXTURE OF BERYLLIUM CONCENTRATES | 2013 |
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RU2561402C2 |
Authors
Dates
2015-04-10—Published
2013-12-11—Filed