MICROCRYSTALLINE CELLULOSE SULPHATION METHOD Russian patent published in 2015 - IPC C08B5/14 

Abstract RU 2558885 C1

FIELD: chemistry.

SUBSTANCE: invention relates to chemical processing of wood and sulphation of microcrystalline cellulose. Water-soluble sulphates of microcrystalline cellulose are widely used as blood anticoagulants, toxic metal sorbents, immunomodulators and antiviral agents. Sulphation of microcrystalline cellulose is carried out with a mixture of sulphamic acid and urea in N,N-dimethyl formamide or diglyme while boiling and stirring intensely for 1-4 hours, and the sulphated microcrystalline cellulose is separated by neutralising the reaction mass with 75% aqueous ethanol solution containing 3% sodium hydroxide, dissolving the obtained product in water and purifying the product by dialysis.

EFFECT: improved method.

2 tbl

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RU 2 558 885 C1

Authors

Levdanskij Vladimir Aleksandrovich

Levdanskij Aleksandr Vladimirovich

Kuznetsov Boris Nikolaevich

Dates

2015-08-10Published

2014-02-10Filed