FIELD: chemistry.
SUBSTANCE: nanosized titanium dioxide is modified with manganese by adding potassium permanganate to the reaction mixture. Ammonia is used as a reducing agent for permanganate ions. Titanyl sulphate solution TiOSO4·2H2O reacts in diluted sulphuric acid with potassium permanganate and ammonia solutions. The reaction mixture is then heated at 80-95°C and HCl is then added. The precipitate is filtered out, washed with water and acetone and then dried on air at room temperature.
EFFECT: invention simplifies the process of producing samples of nanosized titanium dioxide doped with manganese, and reduces the duration and power consumption of the process.
5 dwg, 4 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PREPARING PHOTOCATALYST BASED ON η-MODIFICATION OF VANADIUM-DOPED TITANIUM DIOXIDE, ACTIVE IN VISIBLE SPECTRUM REGION | 2013 |
|
RU2540336C1 |
METHOD OF PREPARING TITANIUM OXIDE PHOTOCATALYST ACTIVE IN VISIBLE SPECTRUM | 2012 |
|
RU2520100C1 |
METHOD OF PRODUCING NANOSIZED TITANIUM DIOXIDE | 2014 |
|
RU2565193C1 |
METHOD FOR OBTAINING PHOTOCATALYSTS ACTIVE IN THE VISIBLE RANGE OF THE SPECTRUM WITH NANOSCALE TITANIUM OXIDES WITH THE STRUCTURE OF ANATASE AND A MIXTURE OF ANATASE AND RUTILE DOPED WITH TRANSITION METALS (Ni, V, Ag, Cu, Mn) | 2021 |
|
RU2776582C1 |
METHOD OF OBTAINING NANOSIZE η-MODIFICATION OF TITANIUM DIOXIDE | 2011 |
|
RU2469954C2 |
PHOTOCATALYST BASED ON NANOSIZED η-MODIFICATION OF TITANIUM DIOXIDE | 2011 |
|
RU2469788C1 |
METHOD OF OBTAINING η-TiO NANOSIZED MODIFICATION | 2014 |
|
RU2576054C1 |
METHOD OF PRODUCING ADSORBENT BASED ON NANOSIZED ANATASE-STRUCTURED TITANIUM DIOXIDE | 2011 |
|
RU2463252C1 |
METHOD FOR PRODUCING PHOTOCATALYTICALLY ACTIVE NANOCRYSTALLINE ANATASE TITANIUM DIOXIDE | 2013 |
|
RU2551677C2 |
METHOD OF PRODUCTION OF PHOTOCATALYTIC SORBING FABRIC MATERIAL | 2014 |
|
RU2559506C1 |
Authors
Dates
2015-10-20—Published
2014-05-20—Filed