FIELD: metallurgy.
SUBSTANCE: invention relates to nanocomposite material production for electrocatalysis, electric sorption, and device for electric energy accumulation. It can be used to produce high effective electrocatalysts, electric sorbents and energy accumulating devices. The method includes electric deposition of polymer matrix during passage of DC with density 1-5 mA/cm2 for 1-5 minutes through layer of finely dispersed deposit of metal oxide or of hydrated metal oxide, that is preliminary deposited on the electrode located on cell bottom, by sedimentation from mixed water-organic solution 0.01-0.1 mol/l of monomer 3,4-ethyldioxythiophen, containing suspended low soluble colloidal forms of metal oxide or powder of metal oxide. Device contains cylindrical electrolyser, inside it secondary electrode 2, reference electrode 3 and work electrode 4 with current lead 6 are located, at that work electrode 4 is detachable bottom of cell, is arranged in insulating enclosure with thread 5 and is tightly connected with cell 1 by nut with thread 7 and gasket 8.
EFFECT: reduced time of production of nanocomposite material due to formation by one stage, increased uniformity of particles distribution in matrix volume.
5 cl, 2 ex, 11 dwg
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