FIELD: chemistry.
SUBSTANCE: invention relates to the method of producing the monohydrate of the compound of formula by treating the compound of formula with the compound of formula in a reaction mixture, followed by treating the dissolved compound of formula (I) with an acid to form the salt of the compound of formula (I), which precipitates from the solution containing the dissolved compound of formula (I), and then treating the said salt of the compound of formula (I) with an aqueous basic solution to precipitate the monohydrate of the compound of formula (I).
EFFECT: improved method.
13 cl, 1 ex
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Authors
Dates
2016-04-20—Published
2011-04-08—Filed