FIELD: chemistry.
SUBSTANCE: invention relates to organic synthesis, particularly to production of tricyclic derivatives of 1-pirazolina, containing 9-13 carbon atoms, an aldehyde group and 5-merous cycle with diaza-group. Method is based on reaction C2-C6 Omega-alkenylboronic norbornene, for example 5-vinyl-2-norbornene with nitrous oxide (N2O) at a temperature of 100-250 °C and total pressure of 2-150 ATM.
EFFECT: it is suggested a single-step method of producing novel tricyclic derivatives of 1-pirazolina appropriate to the formula a, where n = 0÷4.
7 cl, 1 tbl, 1 ex
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Authors
Dates
2016-09-20—Published
2015-06-25—Filed