METHOD FOR SYNTHESIS OF ETHYLENEDIAMINE-N,N,N',N'-TETRAPROPIONIC ACID Russian patent published in 2017 - IPC C07C227/18 C07C229/16 

Abstract RU 2611011 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method for producing ethylenediamine-N,N,N',N'-tetrapropionic acid, used as a complexing agent in analytical chemistry, biology and medical science. The claimed method involves carboxyalkylation of ethylenediamine at an elevated temperature and isolation of the target product. For that purpose, an aqueous solution of acrylic acid is used as a carboxyalkylating agent, heated up to 40-45°C, wherein ethylenediamine is added to the said acid aqueous solution under continuous stirring. The ethylenediamine to acrylic acid molar ratio is 1:4.0-4.4. The reaction mix is stirred at a temperature of 60-65°C, cooled down, and the target product is filtered out.

EFFECT: single-stage method for producing ethylenediamine-N,N,N',N'-tetrapropionic acid with a high purity and high yield product.

4 cl, 4 ex

Similar patents RU2611011C1

Title Year Author Number
ETHYLENEDIAMINE-N,N,N',N'-TETRAPROPIONIC ACID PREPARATION METHOD 2006
  • Tsirul'Nikova Nina Vladimirovna
  • Chicherina Galina Petrovna
RU2308448C1
METHOD OF OBTAINING ASYMMETRIC ETHYLENE DIAMINE-N,N-DIPROPIONIC ACID 2012
  • Podmareva Ol'Ga Nikolaevna
  • Tsirul'Nikova Nina Vladimirovna
  • Fetisova Tat'Jana Sergeevna
  • Starikova Zoja Aleksandrovna
RU2507195C1
METHOD OF PRODUCING ETHYLENEDIAMINE-N-MONOPROPIONIC ACID 2012
  • Tsirul'Nikova Nina Vladimirovna
  • Podmareva Ol'Ga Nikolaevna
  • Fetisova Tat'Jana Sergeevna
RU2489420C1
METHOD FOR PRODUCING ETHYLENEDIAMINE-N-MONOPROPIONIC ACID SULPHATE SALT 2022
  • Tsirulnikova Nina Vladimirovna
  • Fetisova Tatyana Sergeevna
  • Khachatryan Derenik Sarkisovich
  • Poplevin Dmitrij Sergeevich
RU2786854C1
METHOD OF PRODUCING ETHYLENEDIAMINE-N,N'-DI-α-PROPIONIC ACID 2014
  • Tsirul'Nikova Nina Vladimirovna
  • Podmareva Ol'Ga Nikolaevna
  • Dernovaja Elena Sergeevna
  • Belus' Svetlana Konstantinovna
  • Fetisova Tat'Jana Sergeevna
RU2554095C1
METHOD FOR PRODUCTION OF ETHYLENEDIAMINE-N,N'-DIPROPIONIC ACID DIHYDROCHLORIDE 2006
  • Tsirul'Nikova Nina Vladimirovna
  • Tarasova Marina Aleksandrovna
RU2307828C1
METHOD OF PRODUCING ALKYLENE AMINOPOLYCARBOXYLIC ACIDS 2011
  • Zagidullin Rais Nurievich
  • Abdrakhmanov Il'Dus Baryevich
  • Mustafin Akhat Gaziz'Janovich
  • Zagidullina Saira Karimovna
  • Zagidullina Raushan Raisovna
RU2471772C1
METHOD FOR PRODUCING ASYMMETRIC ETHYLENEDIAMINE-N,N-DI(3-PROPIONIC ACID) ZINC COMPLEXATE 2017
  • Tsirulnikova Nina Vladimirovna
  • Dernovaya Elena Sergeevna
  • Fetisova Tatyana Sergeevna
RU2661874C1
ZINC COMPLEX OF ASYMMETRIC ETHYLENEDIAMINE-N,N-DIPROPYONIC ACID DICHLORIDE AND METHOD OF ITS OBTAINING 2012
  • Podmareva Ol'Ga Nikolaevna
  • Tsirul'Nikova Nina Vladimirovna
  • Starikova Zoja Aleksandrovna
  • Fetisova Tat'Jana Sergeevna
RU2511271C2
METHOD OF PRODUCING 1,3-DIAMINO-2-HYDROXYPROPANE-N,N'-DIMETHYLPHOSPHONIC-N,N'-DIACETIC ACID 2015
  • Tsirulnikova Nina Vladimirovna
  • Dernovaya Elena Sergeevna
  • Bolt Yaroslav Vasilevich
  • Fetisova Tatyana Sergeevna
RU2589715C1

RU 2 611 011 C1

Authors

Tsirulnikova Nina Vladimirovna

Volosneva Olga Nikolaevna

Dernovaya Elena Sergeevna

Fetisova Tatyana Sergeevna

Dates

2017-02-17Published

2016-03-30Filed