METHOD FOR PRODUCTION OF ETHYLENEDIAMINE-N,N'-DIPROPIONIC ACID DIHYDROCHLORIDE Russian patent published in 2007 - IPC C07C227/08 C07C229/16 

Abstract RU 2307828 C1

FIELD: organic chemistry.

SUBSTANCE: new two-step method for production of ethylenediamine-N,N'-dipropionic acid in form of dihydrochloride includes reaction of β-chloropropionic acid calcium salt with ethylene diamine in presence of calcium oxide in amount to maintain pH 9-11 and at not higher than 85°C. Then reaction mass is cooled and acidified with concentrated hydrochloric acid to pH 1.0-1.5, held at decreased temperature and finished product is isolated with yield of 40 %. Structure of finished product is suggested by C13 NMR spectra. Compound of present invention is useful as chelating agent in chemistry, agriculture, medicine.

EFFECT: method of increased processability and efficiency, decreased energy consumption.

4 cl, 1 ex

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RU 2 307 828 C1

Authors

Tsirul'Nikova Nina Vladimirovna

Tarasova Marina Aleksandrovna

Dates

2007-10-10Published

2006-04-03Filed