FIELD: chemistry.
SUBSTANCE: continuous distillation column has been installed to organize the continuous flow of the process and ensure the material and heat balance of the flows between the photochemical and catalytic modules allowing efficient separation of components such as norbornadiene and quadricyclan and directing them to the appropriate modules, regulating the cyclicity of the transformations.
EFFECT: increase in quantitative yield quadricyclane, requiring no further purification from the impurities, and the number of cycles to ensure continuity of the process.
3 cl, 2 ex, 2 tbl, 1 dwg
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