FIELD: chemistry.
SUBSTANCE: method for manufacture of zeolitic material with an MFI type framework structure, comprises the steps of: (1) provision of a mixture containing one or more YO2 sources and one or more alcenyltrialkylammonium R1R2R3R4N+ cation containing compounds as a directing agent for structure formation; and (2) crystallization of the mixture obtained in step (1), to give a zeolite material. In this case Y is a tetravalent element. R1, R2 and R3 independently of one another represent n-propyl; and R4 is 2-propen-1-yl or 1-propen-1-yl. Preferably, the directing agent for structure formation introduced in step (1) comprises N-(2-propen-1-yl)-tri-n-propylammonium hydroxide and/or N-(1-propen-1-yl)-tri-n-propylammonium hydroxide.
EFFECT: invention improves method efficiency, providing the possibility of obtained material application as an adsorbent or catalyst.
41 cl, 8 dwg, 7 ex, 5 tbl
Title | Year | Author | Number |
---|---|---|---|
ZEOLITE MATERIALS OF SLEEP TYPE AND METHODS OF THEIR PRODUCTION WITH THE USE OF CYCLOALKYLAMMONIUM COMPOUNDS | 2013 |
|
RU2627399C2 |
ORGANOTEMPLATE-FREE SYNTHETIC PROCESS FOR PRODUCTION OF A ZEOLITIC MATERIAL OF CHA-TYPE STRUCTURE | 2012 |
|
RU2612697C2 |
MOLDING OF A HYDROPHOBIC ZEOLITIC MATERIAL AND PROCESS FOR ITS PRODUCTION | 2014 |
|
RU2670616C2 |
POST-TREATMENT OF DEBORATED ZEOLITE MWW | 2013 |
|
RU2638851C2 |
CHA TYPE ZEOLITIC MATERIALS AND METHODS FOR THEIR PREPARATION USING COMBINATIONS OF CYCLOALKYL- AND TETRAALKYLAMMONIUM COMPOUNDS | 2015 |
|
RU2678676C2 |
ZEOLITE MATERIAL POST-TREATMENT | 2013 |
|
RU2637021C2 |
POST-TREATMENT OF DEBORATED ZEOLITE BETA | 2013 |
|
RU2636724C2 |
METHOD OF PRODUCING ZEOLITE MATERIAL USING ELEMENTARY PRECURSORS | 2013 |
|
RU2636085C2 |
COPPER-PROMOTED GMELINITE AND ITS USE IN SELECTIVE CATALYTIC REDUCTION OF NO | 2017 |
|
RU2740455C2 |
MOLDED PIECE CONTAINING ZEOLITE MATERIAL HAVING MFI FRAME STRUCTURE TYPE | 2019 |
|
RU2808562C2 |
Authors
Dates
2017-06-14—Published
2013-04-24—Filed