METHOD FOR PRODUCING HEXAFLUOROISOPROPANOL AND FLUOROMETHYLGEXAFLUOROISOPROPYL ETHER (SEVOFLURANE) Russian patent published in 2017 - IPC C07C41/01 C07C43/12 C07C29/145 C07C31/38 

Abstract RU 2629366 C2

FIELD: chemistry.

SUBSTANCE: one embodiment of the method for the producing sevoflurane comprises the following steps: (a) purification of a mixture containing hexafluoroacetone and more than 120 ppm of 1,1,1-trifluoro-2,2-dichloroethane as an impurity to produce purified hexafluoroacetone containing 120 ppm or less than 1,1,1-trifluoro-2,2-dichloroethane; (b) reduction of hydrogen (H2) in contact with the purified hexafluoroacetone in the presence of a catalyst, whereby hexafluoroacetone is hydrogenated to give hexafluoroisopropanol, and (c) reaction of hexafluoroisopropanol, formaldehyde and hydrogen fluoride in the presence of the Lewis acid or the Bronsted acid.

EFFECT: reducing the time of receipt.

23 cl, 4 tbl, 25 ex

Similar patents RU2629366C2

Title Year Author Number
METHOD OF OBTAINING HEXAFLUORISOPROPANOL 2007
  • Igumnov Sergej Mikhajlovich
  • Vjazkov Vladimir Arkad'Evich
RU2346924C1
METHOD OF PRODUCING HEXAFLUOROPROPANOL 2011
  • Igumnov Sergej Mikhajlovich
  • Tjutjunov Andrej Aleksandrovich
RU2470005C1
METHOD OF OBTAINING HEXAFLUOROISOPROPANOL 2014
  • Igumnov Sergej Mikhajlovich
  • Sin'Ko Aleksandr Vladimirovich
  • Don Veronika L'Vovna
RU2547654C1
METHOD OF PRODUCING CARBONATE COMPOUND 2008
  • Okamoto Khidekazu
  • Tadzima Koukhej
  • Okazoe Takasi
RU2494088C2
METHOD OF 1,1,1,2-TETRAFLUOROETHANE SYNTHESIS 1991
  • Dzhon Dehvid Skott[Gb]
  • Rechel Anne Stiven[Gb]
RU2007381C1
PROCESS FOR 1,1,1,2-TETRAFLUOROETHANE 1991
  • Dzhon Dehvid Skott[Gb]
  • Rechel Anne Stiven[Gb]
RU2015957C1
METHOD OF EXTRACTION OF HYDROGEN FLUORIDE 1998
  • Ehving Pol Nikolas
  • Lou Robert Ehlliott
  • Shildz Charl'Z Dzhon
RU2194007C2
METHOD OF HYDROGENOLYSIS AND/OR DEHYDROHALOGENATION OF FLUOROHALOCARBONS AND/OR FLUOROHALOHYDROCARBONS 1991
  • Karl Stiven Kellner[Us]
  • V.N.Mallikardzhuna Rao[Us]
  • Frehnk Dzhuliehn Vejgert[Us]
RU2026279C1
METHOD OF PREPARING HEXAFLUOROACETONE 1998
  • Igumnov S.M.
  • Shipigusev A.A.
  • Lekontseva G.I.
  • Soshin V.A.
RU2156756C2
METHOD OF PREPARING HEXAFLUOROACETONE 0
  • Vilenchik Yakov Moiseevich
  • Yakurnova Galina Ivanovna
  • Lekontseva Galina Ivanovna
  • Zayakina Lyubov Pavlovna
  • Kharchenko Aleksej Pavlovich
SU740741A1

RU 2 629 366 C2

Authors

Morino Yuzuru

Fujii Shigeru

Nakamichi Toshihiro

Akiba Shinya

Takeda Masaaki

Fujiwara Masaki

Dates

2017-08-29Published

2016-12-02Filed