METHOD OF PRODUCING HEXAFLUOROPROPANOL Russian patent published in 2012 - IPC C07C31/38 C07C29/143 

Abstract RU 2470005 C1

FIELD: chemistry.

SUBSTANCE: method involves reducing hexafluoroacetone (HFA) in an aqueous medium, wherein the hexafluoroacetone is used in trihydrate form or 50% aqueous solution, and the reducing agent used is phosphorous acid in the presence of aqueous ammonia solution in molar ratio HFA:H3PO3NH3 (1:1.2-1.3:3), with catalysis by transition metal salts.

EFFECT: invention enables to obtain the end product in a single step using cheap and nontoxic reactants.

2 ex, 1 tbl

Similar patents RU2470005C1

Title Year Author Number
METHOD OF OBTAINING HEXAFLUOROISOPROPANOL 2014
  • Igumnov Sergej Mikhajlovich
  • Sin'Ko Aleksandr Vladimirovich
  • Don Veronika L'Vovna
RU2547654C1
METHOD OF OBTAINING HEXAFLUORISOPROPANOL 2007
  • Igumnov Sergej Mikhajlovich
  • Vjazkov Vladimir Arkad'Evich
RU2346924C1
METHOD FOR PRODUCING HEXAFLUOROISOPROPANOL AND FLUOROMETHYLGEXAFLUOROISOPROPYL ETHER (SEVOFLURANE) 2016
  • Morino Yuzuru
  • Fujii Shigeru
  • Nakamichi Toshihiro
  • Akiba Shinya
  • Takeda Masaaki
  • Fujiwara Masaki
RU2629366C2
METHOD FOR SYNTHESISING PENTAFLUOROPROPIONIC ACID 2020
  • Igumnov Sergej Mikhajlovich
  • Sinko Aleksandr Vladimirovich
  • Molchanov Maksim Dmitrievich
RU2758675C1
METHOD OF PREPARING HEXAFLUOROACETONE 1998
  • Igumnov S.M.
  • Shipigusev A.A.
  • Lekontseva G.I.
  • Soshin V.A.
RU2176997C2
METHOD OF PREPARING HEXAFLUOROACETONE 1998
  • Igumnov S.M.
  • Shipigusev A.A.
  • Lekontseva G.I.
  • Soshin V.A.
RU2156756C2
METHOD OF PRODUCING 2-(4-HYDROXY-MORPHOLINYL)-2-CYCLOHEXENONE 2007
  • Napolitano Ehlio
RU2439066C2
METHOD FOR THE PRODUCTION OF N-HYDROXY MORPHOLINE 2020
  • Kondratev Vladimir Borisovich
  • Malenkov Mikhail Yurevich
  • Kaabak Leonid Vladimirovich
  • Golikov Aleksej Gennadevich
  • Golovkov Vladimir Fedorovich
RU2757983C1
SYNTHESIS OF 5-METHYL-2-PROPIONYLFURAN 2005
  • Germanov Sergej Borisovich
RU2282626C1
METHOD OF PRODUCTION OF NITRILOTRIMETHYLENEPHOSPHONIC ACID 2023
  • Beev Aues Akhmedovich
  • Khashirova Svetlana Iurevna
  • Daov Ruslan Iurevich
  • Beeva Dzhuletta Anatolevna
RU2811397C1

RU 2 470 005 C1

Authors

Igumnov Sergej Mikhajlovich

Tjutjunov Andrej Aleksandrovich

Dates

2012-12-20Published

2011-12-09Filed