FIELD: chemistry.
SUBSTANCE: oxide-nickel catalyst production method includes the impregnating of alumina-based carrier with the nickel nitrate solution, further drying at the temperature of 100-120°C and calcination at the temperature of 450-500°C. The method is characterized in that, the carrier is preliminarily impregnated with the ammonia-carbonate solution with the concentration of NH3 - 31-40 g/l, CO2 - 81-90 g/l. Then, the carrier is washed with distilled water and the single hydrothermal treatment is carried out in the solution of nickel nitrate with the concentration of 100-300 g/l at the temperature of 50-80°C for 2-4 hours. In the method, the thickness of the surface catalytically active layer is formed as necessary within the range of 350-650 mcm.
EFFECT: oxide-nickel catalyst production method creation on the inert carrier with the controlled thickness of the surface oxide-nickel layer in the industrial volumes, the method is characterized by the reduction of the catalyst production technological stages number and the increase of its service life.
2 cl, 4 dwg, 5 ex
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Authors
Dates
2017-09-15—Published
2016-09-06—Filed