FIELD: chemistry.
SUBSTANCE: invention relates to a method for preparation of a sulphylimine compound, such as N-cyano-S-methyl-S-[1-(6-trifluoromethyl-3-pyridinyl)ethyl]sulfinylimine, or another substituted sulphylimine compound which includes reaction of a sulfide compound, cyanamide, hypochlorite and base, and sulphide compound oxidizing to produce a sulphylimine compound. A buffer compound, such as a phosphate buffer, may be optionally used in the reaction.
EFFECT: method improvement.
17 cl, 4 tbl, 4 ex
Title | Year | Author | Number |
---|---|---|---|
PYRIDINE-N-OXIDES AND PROCESSES FOR THEIR PREPARATION | 2013 |
|
RU2628339C2 |
INSECTICIDUM N-SUBSTITUTED SULPHYLIMINES AND SULPHOXIMINES OF N-PYRIDINE OXIDES | 2013 |
|
RU2639870C2 |
COMPOUNDS AND COMPOSITIONS AS ITPKb INHIBITORS | 2007 |
|
RU2425826C2 |
HETEROCYCLIC COMPOUNDS AND THEIR APPLICATION AS GLYCOGEN SYNTHASE KINASE-3 INHIBITORS | 2011 |
|
RU2623427C2 |
ISOXAZOLINE DERIVATIVE AND HERBICIDE COMPRISING ITS AS ACTIVE COMPONENT | 2002 |
|
RU2286989C2 |
APPLICATION OF ARYL AND HETARYL CARBOXAMIDES AS ENDOPARASITICIDES | 2012 |
|
RU2638830C2 |
METHOD FOR PREPARING DERIVATIVES OF 2-AMINO-4-CHLORO-1,3,5-TRIAZINES | 1999 |
|
RU2271353C2 |
IMIDAZOPYRIMIDINE DERIVATIVES AS MODULATORS OF TNF ACTIVITY | 2014 |
|
RU2691629C1 |
TETRAHYDROIMIDAZOPYRIDINE DERIVATIVES AS TNF ACTIVITY MODULATORS | 2014 |
|
RU2684635C1 |
TETRAHYDROIMIDAZOPYRIDINE DERIVATIVES AS MODULATORS OF TNF ACTIVITY | 2014 |
|
RU2696270C1 |
Authors
Dates
2017-11-03—Published
2013-02-15—Filed