FIELD: chemistry.
SUBSTANCE: proposed method includes the catalytic oxidation of cis-cyclooctene by molecular oxygen in the liquid phase at atmospheric pressure and at the temperature of 100-130°C. Oxidation is carried out using a catalytic system comprising an organic or inorganic molybdenum compound and a phthalimide compound (N-hydroxyphthalimide, 4-methyl-N-hydroxyphthalimide, 4-phenyl-N-hydroxyphthalimide) in the amount of 0.2-0.4 wt %, at the ratio of the components of the catalytic system (molybdenum compound: phthalimide compound) 1:1÷10.
EFFECT: increasing the selectivity of production and reducing the number of by-products.
3 ex
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| METHOD OF PRODUCING EPOXIDE OF DICYCLOPENTENE (EPOXIDE OF TRICYCLO-[5,2,1,0]DECENE-3,9-OXATETRACYCLO-[5,3,1,0,0]-UNDECANE) | 2011 |
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