FIELD: chemistry.
SUBSTANCE: invention refers to a method of obtaining a compound (1) used as a contrast agent for carrying out radiological studies, from the compound (3). In the compound (3), each X individually represents hydrogen, a formyl group (-CO-H) or an acetyl group (-CO-CH3). The method includes a base-activated in situ hydrolysis of the protecting groups (-OX) of the compound (3), comprising the following successive steps: i) suspending the compound (3) in water; ii) adjusting the pH of the solution obtained in step i) to a value between 10.0 and 12.5.
EFFECT: method makes it possible to shorten the reaction time and increase the yield of the compound.
6 cl, 1 ex
| Title | Year | Author | Number |
|---|---|---|---|
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| METHOD FOR PRODUCING INJECTED CONTRAST MEDIUM | 0 |
|
SU1829940A3 |
