FIELD: chemistry.
SUBSTANCE: method of producing chelated S,S-dimiodi (I) bis [(3,5-dimethylisoxazol-4-yl)methylsulfanyl]ethane dichloride complex with the general formula . The method comprises reacting 1,2-bis [sulfonylmethyl (3,5-dimethylisoxazol-4-yl)]ethane with dimiodi dichloride (I) in acetonitrile at a molar ratio of bis [sulfonylmethyl (3,5-dimethylisoxazol-4-yl)]ethane: dimedi (I) dichloride, equal to 1:0.5, at a temperature of 55-70°C and atmospheric pressure for 2-4 hours.
EFFECT: invention makes it possible to produce the said complex, which can be used as a catalyst for chemical reactions.
1 dwg,1 tbl, 1 ex
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RU2780151C1 |
Authors
Dates
2018-05-16—Published
2016-04-26—Filed