FIELD: biotechnology; technological processes.
SUBSTANCE: invention relates to organic synthesis and relates to processes for the preparation of 1-nitronaphthalene. Object of the invention is to carry out nitration in homogeneous conditions. 1-nitronaphthalene is formed by the reaction of naphthalene dissolved in dioxane with a nitrating mixture consisting of concentrated sulfuric and concentrated nitric acids. Nitration is carried out with stirring and heating in a boiling water bath for 40–60 minutes. Yield of 1-nitronaphthalene reaches 97 % of the theoretical yield.
EFFECT: proposed solution allows for synthesis under homogeneous conditions.
5 cl, 1 tbl, 8 ex
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