FIELD: technological processes; chemistry.
SUBSTANCE: invention can be used for the chemical-thermal treatment of the inner cylindrical surface of structural materials and products of low- and high-alloy steels, titanium and titanium alloys. Article is placed in a vacuum chamber. Argon is introduced into the vacuum chamber and the surface is pretreated with a pulse-periodic anomalous glow discharge, after which the product is heated to a temperature above 150 °C by means of an additional heating system. Carry out working gas puffing to a pressure of 0.5–5.0 Torr. Use a mixture of hydrogen and nitrogen or a mixture of hydrogen, nitrogen and argon for steel, and a mixture of argon and nitrogen or a mixture of helium and nitrogen for titanium and its alloys. Nitridizing is carried out in the plasma of a pulse-periodic anomalous glow discharge with a hollow cathode with heating of the surface of the article from steel to 400–650 °C, and articles made of titanium and its alloy up to 400–900 °C by means of an additional heating system. Then, nitrogen is introduced into the vacuum chamber and the article is cooled to a temperature of 25 °C under a nitrogen atmosphere at a high pressure of 800 Torr.
EFFECT: method provides an increase in hardness and corrosion resistance of parts with an internal cylindrical surface with a diameter of 3 mm.
1 cl, 3 ex, 5 dwg
Title | Year | Author | Number |
---|---|---|---|
METHOD OF ION-PLASMA NITRIDING OF ARTICLES FROM TITANIUM OR TITANIUM ALLOY | 2018 |
|
RU2686975C1 |
PROCEDURE FOR PLASMA NITRIDING ITEM OUT OF STEEL OR NON-FERROUS ALLOY | 2009 |
|
RU2413033C2 |
INTENSIFICATION METHOD OF LOW-TEMPERATURE ION NITRIDING OF ITEMS FROM TITANIUM ALLOYS | 2019 |
|
RU2717124C1 |
METHOD FOR LOW-TEMERATURE ION NITRIDING OF TITANIUM ALLOYS WITH CONSTANT PUMPING OF A GAS MIXTURE | 2018 |
|
RU2687616C1 |
MODIFICATION METHOD OF SURFACE OF ITEMS FROM TITANIUM ALLOYS IN VACUUM | 2014 |
|
RU2562185C1 |
METHOD FOR FORMATION OF TRIBOLOGICAL COATING | 2018 |
|
RU2712661C1 |
PROCEDURE FOR FORMING NON-UNIFORM STRUCTURE OF MATERIAL AT NITRIDING IN GLOW DISCHARGE | 2009 |
|
RU2409699C1 |
METHOD OF COMBINED PLASMA SURFACE TREATMENT OF ITEMS FROM TITANIUM ALLOYS | 2017 |
|
RU2671026C1 |
ION-PLASMA PRECISION NITRIDING OF METAL PART SURFACE | 2013 |
|
RU2555692C2 |
METHOD FOR ION NITRIDING OF PRODUCTS MADE OF CONSTRUCTION ALLOY STEELS | 2020 |
|
RU2760309C1 |
Authors
Dates
2018-11-01—Published
2017-08-14—Filed