FIELD: medicine.
SUBSTANCE: group of inventions relates to a film-forming powder for forming a layer on a tooth surface, a method of producing such a powder and a granule based on such a powder. Disclosed is a film-forming powder for sputtering on the tooth surface to form a layer on the tooth surface for use in a sputtering device for a tooth with average particle size of 0.5 to 30 mcm. Film-forming powder is obtained by calcining apatite represented by formula Ca10-X⋅MX(ZO4)6Y2, where X corresponds to value from 0 to 10; M represents an element selected from the group: sodium, lithium, magnesium, barium, strontium, zinc, cadmium, lead, vanadium, silicon, germanium, iron, arsenic, manganese, aluminium, rare-earth elements, cobalt, silver, chrome, antimony, tungsten and molybdenum, or hydrogen; ZO4 represents PO4; and Y is a hydroxyl group, a halogen element or a carbonate group, in an inert gas medium at temperature of 600 to 1350 °C. To produce the powder, hydroxyapatite, which is the main component of the tooth, particularly hydroxyapatite with an admixture of a colour shade, can be used. Also disclosed is a method of producing a film-forming powder used in a sputtering device for tooth-spraying on a tooth surface to form a layer on the surface of the tooth with average particle size of 0.5–30 mcm, including the above steps, followed by grinding and sorting. Method can additionally involve exposure to plasma or exposure to plasma and application of mechanical energy. Invention covers also tooth for sputtering on surface of tooth for formation of layer on surface of tooth for use in jet device for tooth containing said film-forming powder.
EFFECT: use of the group of inventions enables to quickly form on the tooth surface a layer with high hardness and extremely low acid solubility by spraying the film-forming powder by means of a spraying device.
19 cl, 82 tbl, 10 ex, 9 dwg
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Authors
Dates
2019-05-20—Published
2016-07-12—Filed