FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing isomers of N,N,N-tributyl-N-(3-chloroprop-2-en-1-yl)ammonium chloride based on quaternization of tributylamine with individual isomers of 1,3-dichloropropene or a mixture thereof. Alkylation of tributylamine is carried out in boiling acetonitrile in the presence of catalytic amounts of KI.
EFFECT: higher output of products – 84–85 % on initial tributylamine (in prototype 74–76 %) and reduced duration of process.
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Authors
Dates
2019-05-22—Published
2018-12-06—Filed