METHOD OF MAKING INORGANIC PEROVSKITE NANOWHISKERS OF CsPbBr TYPE Russian patent published in 2019 - IPC C30B29/62 C30B29/12 C01D3/10 C01G21/16 C01D17/00 B82B3/00 B82Y20/00 B82Y40/00 

Abstract RU 2705082 C1

FIELD: nanotechnologies.

SUBSTANCE: invention relates to synthesis of nanostructures based on perovskites, which can be used as materials for nanophotonics to create Fabry-Perot nanosensors and photonic integrated circuits. Method for making insulated perovskite nanowhiskers CsPbBr3 includes treatment of a glass substrate by polishing its surface with a mixture of chromium oxide Cr2O3 particles with diameter less than 100 nm, glyceryl tristearate and oleic acid to create hydrophobic layer, followed by applying a solution of precursors of perovskite CsBr and PbBr2 to the substrate by spraying or spin-coating with formation of solution droplets, then substrate with said application is placed on bottom of vessel, placed in another vessel of larger size, which contains azeotrope: isopropyl alcohol-water (IPA⋅H2O) and is at constant temperature of 50 °C, closing it with a cover and for final formation of nanowhiskers drying is carried out for 5–7 minutes until complete drying of solution drops.

EFFECT: faster operation (production time reduced to 5–7 minutes), simplification and cheapening of manufacturing technology of high-quality inorganic perovskite nanowhiskers of CsPbBr3 type with a longitudinal dimension of 2–50 mcm and a cross section of less than 1 mcm, characterized by low concentration of defect conditions, improved reflectivity of side surfaces and improved optical properties: high Q-factor Q=1,017–6,166 and low generation threshold Pthres=13 nJ/cm2.

1 cl, 6 dwg, 1 ex

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RU 2 705 082 C1

Authors

Pushkarev Anatolij Petrovich

Markina Darya Igorevna

Korolev Vyacheslav Igorevich

Makarov Sergej Vladimirovich

Dates

2019-11-01Published

2018-12-20Filed