METHOD FOR SYNTHESIS OF QUANTUM DOTS OF PEROVSKITE CsPbBr USING MICROWAVE HEATING Russian patent published in 2024 - IPC C30B29/12 C09K11/55 C09K11/61 C09K11/66 B82Y40/00 

Abstract RU 2822107 C1

FIELD: chemistry.

SUBSTANCE: invention relates to chemical industry and can be used in making technically complex semiconductor devices. Into beakers with capacity of 50 ml are loaded precursors – PbBr2 and CsBr in molar ratio 1:1, 2 ml of oleic acid and a solvent, which is 10 ml of dodecane, as well as 0.2 g of octadecylamine. Said substances are mixed. Molar concentration of PbBr2 and CsBr in the mixture is in range of 0.1 to 0.5 mmol/l. Obtained mixture is placed in a microwave oven, heated therein at 700 W for 5 minutes, then cooled to room temperature. Obtained nanoparticles, which are perovskite quantum dots, are centrifuged at 9,000 rpm for 10 minutes to remove supernatant, and the obtained products are dispersed with dodecane for the following experiments.

EFFECT: invention provides high quantum yield of fluorescence of quantum dots and narrowing of their size distribution.

1 cl, 2 dwg

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RU 2 822 107 C1

Authors

Kinev Vladislav Aleksandrovich

Ilina Nadezhda Olegovna

Nazmitdinov Rashid Giiasovich

Mukhina Irina Vladimirovna

Novikova Sagila Aladdinovna

Dates

2024-07-01Published

2023-11-02Filed