FIELD: chemistry.
SUBSTANCE: present invention relates to a method for producing a molecular sieve with an AEI framework. The method for producing a zeolite includes formation a reaction mixture containing one or more sources of silica, one or more sources of alumina, a base and one or more organic structure-directing agents (SDAs) wherein at least part of the source of alumina is a zeolite of the FAU topological type and wherein the reaction mixture comprises less than 600 moles of water per mole of alumina, and interaction of the reaction mixture at a temperature of approximately 75 to approximately 220°C for 0.1 to 20 days to form zeolite crystals with an AEI framework and a silica to alumina ratio (SAR) from approximately 10 to approximately 30, wherein the relative yield based on the ratio of the AEI mass to the reaction mixture mass is approximately ≥ 5% and wherein the components of the reaction mixture are present in specified ratios where the end points are included in the ranges: SiO2Al2O3 - 10 to 100, OH-/SiO2 - 0.2 to 0.9, SDA/SiO2 - 0.01 to 0.2, alkali metal cation/SiO2 - 0.20 to 1.0, H2O/SiO2 - 4 to 60.
EFFECT: technical result of the invention is increased AEI yield relative to the reaction mixture mass ("AEI yield") and increased relative yield of SDA used during synthesis of the AEI zeolite.
11 cl, 6 tbl
Title | Year | Author | Number |
---|---|---|---|
SYNTHESIS OF AEI AND CU-AEI ZEOLITES | 2017 |
|
RU2743043C2 |
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SYNTHESIS OF ZEOLITE WITH FLUORIDE SOURCE | 2017 |
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RU2772154C2 |
AEI HIGH-SILICA ZEOLITE | 2017 |
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RU2746017C2 |
SYNTHESIS OF AN AEI-TYPE ZEOLITE | 2014 |
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RU2764725C2 |
AEI ZEOLITE SYNTHESIS | 2014 |
|
RU2672744C2 |
SCR CATALYST | 2014 |
|
RU2765730C2 |
SCR CATALYST | 2014 |
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RU2697482C1 |
CATALYST FOR TREATING EXHAUST GASES | 2014 |
|
RU2675821C2 |
CATALYST FOR EXHAUST GAS PROCESSING | 2014 |
|
RU2771714C2 |
Authors
Dates
2021-06-21—Published
2016-11-11—Filed