FIELD: powder metallurgy.
SUBSTANCE: invention is related in particular to manufacturing nanostructured thermoelectric materials (TEM). It can be used to make thermoelements. TEM based on Bi2Te3, or Sb2Te3, or PbTe, or GeTe, or SiGe is synthesized by direct fusion of the main components, taken in a stoichiometric ratio, with addition of alloying components. Synthesized TEM is ground using a high-energy planetary ball mill with a grinding ball diameter of 5 mm and a mass ratio of balls to TEM of 10:1 to obtain a nanodispersed powder with a predominance of particles from 10 to 100 nm. Powder compaction is carried out by spark plasma sintering.
EFFECT: increase of thermoelectric quality, mechanical strength of TEM, expansion of operating temperature range.
1 cl, 8 dwg, 6 tbl
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Authors
Dates
2023-04-17—Published
2022-08-29—Filed