METHOD OF PRODUCING POLYETHERSULPHONE Russian patent published in 2025 - IPC C08G75/23 

Abstract RU 2839480 C1

FIELD: chemistry.

SUBSTANCE: present invention relates to a method of producing polyethersulphone. Method of producing polyethersulphone involves the following steps: a. mixing 4,4'-dioxydiphenylsulphone (DODPS), potassium carbonate and aprotic solvent to obtain mixture 1; b. obtaining mixture 2 at the boiling point of the aprotic solvent under conditions of distillation of a mixture of solvent and water; c. mixing mixture 2 with 4,4'-dichlorodiphenylsulphone (DCDPS) and an aprotic solvent at the boiling point of the aprotic solvent under conditions of distillation of a mixture of solvent and water to obtain mixture 3; d. holding mixture 3 at the boiling point of the aprotic solvent under conditions of distillation of the mixture of solvent and water with viscosity of mixture 3, which is not more than 25 Pa*s for up to 49%, inclusive, of the total holding time, as well as not less than 26 Pa*s for 50% inclusive of total holding time, to produce a mixture; e. separating polyethersulphone from the mixture to obtain polyethersulphone; f. drying polyethersulphone to obtain polyethersulphone. Weight ratio of polyethersulphone at step c) and d) ranges from 50.5 to 53.5%.

EFFECT: polyethersulphone obtained using this method has a viscosity number in dimethyl acetamide at 40 °C from 58.6 to 71.6 ml/g, as well as weight-average molecular weight from 85,340 to 104,300 g/mol.

17 cl, 1 dwg, 3 ex

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RU 2 839 480 C1

Authors

Andreeva Tatyana Ivanovna

Gurenkov Vladimir Mikhajlovich

Prudskova Tatyana Nikolaevna

Shibaeva Polina Alekseevna

Rebikov Oleg Vyacheslavovich

Serebryakova Anna Aleksandrovna

Chivanova Larisa Yulevna

Chirkin Andrej Borisovich

Bogoyavlenskaya Ekaterina Vasilevna

Igasheva Varvara Petrovna

Dates

2025-05-05Published

2024-07-12Filed