METHOD OF SYNTHESIS OF PROPARGYL ALCOHOL Russian patent published in 1995 - IPC

Abstract SU 1832674 A1

FIELD: organic chemistry, alcohols. SUBSTANCE: process is carried out by interaction of paraform and acetylene in the presence of catalyst - alkaline metal hydroxide (preferably KOH or NaOH) promoted with equimass mixture of alkaline metal (preferably potassium or sodium formate) and methanol taken at concentration 0.45-5.4% of catalyst mass at molar ratio of catalyst: paraform (0.3-4):1 in the medium of aprotonic nonhydroxylic polar solvent at 0-35 C. Method ensures to decrease explosive hazard of process, yield of product is 65-95.8% , to decrease solvent used consumption from mass ratio paraform:solvent 1:20 to 1:10. EFFECT: simplified process. 2 cl

Similar patents SU1832674A1

Title Year Author Number
0
  • Vilenchik Yakov Moiseevich
  • Soshin Vladimir Aleksandrovich
  • Zayakina Lyubov Pavlovna
  • Kharchenko Aleksej Pavlovich
SU548594A1
METHOD OF PRODUCING METHYL FORMATE, TRACED WITH STABLE CARBON ISOTOPE C 2015
  • Kron Tatjana Evgenevna
  • Noskov Jurij Gennadevich
  • Bolotov Pavel Mikhajlovich
  • Korneeva Galina Aleksandrovna
RU2602081C1
METHOD OF PRODUCING ALKYLARYL(HETARYL)ETHYNYL CARBINOLS 2012
  • Shmidt Elena Jur'Evna
  • Bidusenko Ivan Anatol'Evich
  • Protsuk Nadezhda Il'Inichna
  • Mikhaleva Al'Bina Ivanovna
  • Trofimov Boris Aleksandrovich
RU2479565C1
PROCESS FOR PREPARING 3-METHYLPYRIDINE 0
  • Yusupov Dilmurat
  • Kuchkarov Akhmed Baratovich
  • Akhmerov Kudrat Muftaevich
  • Ismailova Lola Anvarovna
  • Davranov Abdurashid Alievich
SU1049483A1
2-PHENYLPYRROLE SYNTHESIS METHOD 2009
  • Trofimov Boris Aleksandrovich
  • Mikhaleva Al'Bina Ivanovna
  • Sobenina Ljubov' Nikolaevna
  • Petrova Ol'Ga Vital'Evna
RU2397974C1
METHOD OF ETHRIOL OBTAINING 2014
  • Marochkin Dmitrij Vjacheslavovich
  • Kron Tat'Jana Evgen'Evna
  • Karchevskaja Ol'Ga Georgievna
  • Korolev Jurij Aleksandrovich
  • Noskov Jurij Gennad'Evich
  • Korneeva Galina Aleksandrovna
RU2560156C1
METHOD OF PRODUCING 2,6-DI-TERT-BUTYL-4-METHOXYMETHYLPHENOL 2014
  • Alekseeva Ol'Ga Aleksandrovna
  • Akhmed'Janova Raisa Akhtjamovna
  • Liakumovich Aleksandr Grigor'Evich
  • Cherezova Elena Nikolaevna
RU2555709C1
METHOD FOR PREPARING 4,5,6,7-TETRAHYDROINDOLE 2005
  • Trofimov Boris Aleksandrovich
  • Mikhaleva Al'Bina Ivanovna
  • Shmidt Elena Jur'Evna
  • Rjapolov Oleg Alekseevich
  • Platonov Vladimir Borisovich
RU2297410C2
ATOM-ECONOMIC WASTE-FREE METHOD OF PRODUCING 2-(4-FLUORPHENYL)-BUT-3-IN-2-OLA 2016
  • Trofimov Boris Aleksandrovich
  • Shmidt Elena Yurevna
  • Protsuk Nadezhda Ilinichna
RU2629024C1
METHOD OF PRODUCING METHYL FORMATE 2007
  • Novikov Oleg Nikolaevich
RU2377232C2

SU 1 832 674 A1

Authors

Trofimov B.A.

Mikhaleva A.I.

Nesterenko R.N.

Sobenina L.N.

Stankevich V.K.

Voronkov M.G.

Dates

1995-02-27Published

1989-02-13Filed