FIELD: production of high-purity aluminum. SUBSTANCE: product- aluminum alcoholates of formula I Al/OR/3, wherein R- C4-C8 alkyl. Selectivity 99.05-99.95 % . Reagent 1: metallic aluminum. Reagent 2- aliphatic C4-C8 alcohol containing 0.1-9.5 % by weight of water. Reaction conditions: addition of reagent 2 at rate which allows the temperature conditions to maintain not less than 165 C followed by evaporation of water containing in alcohol at a time as azeotrope due to exothermic alcoholysis reaction. EFFECT: enhanced efficiency. 1 tbl
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Authors
Dates
1994-01-15—Published
1990-08-22—Filed