FIELD: organic chemistry. SUBSTANCE: product: derivatives of 4-oxo-3H-phthalazine-1-acetic acid of the general formula I, , where R1 - C1-C6-alkyl - are intermediate compounds. Products of the general formula II (image), where R1 - C1-C6-alkyl; R2 and R3 are similar or different and mean hydrogen, fluorine, chlorotrifluoromethyl. Reagent 1 - according to formula III, , where W - CN-group or C(S)NH2. Reagent 2 - according to formula IV, (R2, R3)C6H2-NO2-Cl (IV). Reaction conditions: hydrogen sulfide, tertiary amine. EFFECT: improved method of synthesis. 3 cl
Authors
Dates
1994-06-15—Published
1990-05-10—Filed