DERIVATIVE OF 4-OXO-3H- PHTHALAZINE -1-ACETIC ACID, A METHOD OF SYNTHESIS OF 4-OXO-3H- PHTHALAZINE-1- ACETIC ACID ALKYL ESTER DERIVATIVES Russian patent published in 1994 - IPC

Abstract RU 2014333 C1

FIELD: organic chemistry. SUBSTANCE: product: derivatives of 4-oxo-3H-phthalazine-1-acetic acid of the general formula I, , where R1 - C1-C6-alkyl - are intermediate compounds. Products of the general formula II (image), where R1 - C1-C6-alkyl; R2 and R3 are similar or different and mean hydrogen, fluorine, chlorotrifluoromethyl. Reagent 1 - according to formula III, , where W - CN-group or C(S)NH2. Reagent 2 - according to formula IV, (R2, R3)C6H2-NO2-Cl (IV). Reaction conditions: hydrogen sulfide, tertiary amine. EFFECT: improved method of synthesis. 3 cl

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RU 2 014 333 C1

Authors

Banavara Lakshmana Milari[Us]

Vill'Jam Dzhejms Zembrovski[Us]

Dates

1994-06-15Published

1990-05-10Filed