FIELD: processes for preparing crystalline zeolite alumosilicates. SUBSTANCE: a reaction mixture is subjected to hydrothermal crystallization. The reaction mixture contains SiO2 and Al2O3 sources, mineral substances and crystalline nuclei in an aqueous alkali medium, the molar ratios being as follows: SiO2/Al2O3 20-60; OH-/SiO2 0.10 - 0.20; and H2S/SiO2 20 - 60. The hydrothermal crystallization is carried out in two stages: the first stage covers a temperature range of 245-325 C for 1-20 min; the second stage covers a temperature range of 120-225 C for 1-100 hr. EFFECT: greater efficiency of the process.
Title | Year | Author | Number |
---|---|---|---|
METHOD OF PREPARING OF ZEOLITE ALUMINOSILICATES WITH MOLAR RATIO SiO/AlO= 20 | 1990 |
|
RU2026815C1 |
METHOD FOR PRODUCTION OF SYNTHETIC CRYSTALLINE ALUMINOSILICATE | 1990 |
|
RU2066675C1 |
SYNTHETIC CRYSTALLINE ALUMOSILICATE | 1991 |
|
RU2042621C1 |
METHOD OF PREPARING CRYSTALLINE GALLOSILICATE WITH ZEOLITE STRUCTURE AND ATOMIC RATIO Si/Ga ≥ 5 | 1991 |
|
RU2044690C1 |
METHOD OF PRODUCING GALLIUM SILICATE AT ATOMIC RATIO SI/GA Si/σa ≥ 20 = 20 | 1991 |
|
RU2041860C1 |
METHOD OF CATALYTIC ISOMERIZATION OF C AROMATIC HYDROCARBONS | 1991 |
|
RU2094419C1 |
METHOD FOR MODIFIED ZEOLITE PRODUCTION | 0 |
|
SU1799354A3 |
SYNTHETIC CRYSTALLINE ALUMINOSILICATE AS CATALYST COMPONENT FOR CATALYTIC CONVERSION OF HYDROCARBONS | 1994 |
|
RU2083281C1 |
CRYSTALLINE ZEOLITE-LIKE GALLOSILICATE, METHOD OF ITS SYNTHESIS AND CATALYST BASE FOR HYDROCARBON CONVERSION | 1992 |
|
RU2076845C1 |
PARTIALLY CRYSTALLINE TRANSIENT ALUMINIUM OXIDE, METHOD OF ITS PRODUCING AND METHOD OF PRODUCING THE FORMED $$$-ALUMINIUM OXIDE FROM IT | 1992 |
|
RU2078043C1 |
Authors
Dates
1994-08-30—Published
1990-06-08—Filed