FIELD: organic chemistry. SUBSTANCE: product: derivatives of 6,7-dihydro-5H-dibenz[c,e]azepine-7-one of the general formula where R - F or Cl. Reagent 1: substituted benzoyl chloride. Reagent 2: 6,7-dihydro-5H-dibenz[c,e]azepine-7-one. Reagent 3: pyridine. Reaction conditions: boiling with reflux condenser for 4 h at 120 C. EFFECT: improved method of synthesis.
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Authors
Dates
1995-01-27—Published
1991-06-17—Filed