FIELD: organic chemistry. SUBSTANCE: desired product has formula (CH3)3Si-O-Si(CH3)3, its essential formula being C6H18OSi2. (CH3)3Si-NH-Si(CH3)3 is used as reagent 1, HCl together with H2O are used as reagent 2. Reaction is carried out at 75-90 C, pH being 6-7 and 7.5-5.5. EFFECT: improves efficiency of the method.
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Authors
Dates
1995-04-10—Published
1992-06-03—Filed