FIELD: organic compounds. SUBSTANCE: 1,1-dichlor-1-fluoroethane is used as reagent 1, anhydrous HF being used as reagent 2. Reaction is carried out at 55-95 C in vapor phase, molar ratio of said reagents being 1:4-1:8. Aluminium fluoride being prepared by treatment of anhydrous aluminium chloride or aluminium oxide with hydrogen fluoride is used as catalyst. Desired product having essential formula CH3CCl2F and boiling point 32 C is prepared at yield 99.8 %. EFFECT: improves efficiency of method.
| Title |
Year |
Author |
Number |
| METHOD OF SYNTHESIS OF 1,1-DICHLORO-1-FLUOROETHANE AND A METHOD OF 1,1-DICHLOROETHYLENE CONTENT DECREASE |
1990 |
- Stiven Genri Svirindzhen[Us]
- Dzhon Frehnsis Vekhner[Us]
- Marlin Grajer Ridli[Us]
|
RU2024474C1 |
| PROCESS FOR PREPARING 1,1,1-TRIFLUORODICHLOROETHANE AND/OR 1,1,1,2-TETRAFLUOROCHLOROETHANE |
1990 |
- Leo E.Manzer[Us]
- V.N.Mallikardzhuna Rao[Us]
|
RU2015956C1 |
| METHOD FOR PRODUCTION OF FLUOROMETHANES OR FLUOROETHANES |
1990 |
- V.N.Mallikardzhuna Rao[Us]
|
RU2043985C1 |
| METHOD OF FLUORINATED ALKANES SYNTHESIS |
1990 |
- V.N.Mallikardzhuna Rao[Us]
|
RU2021246C1 |
| METHOD OF FLUORINATED ALKANES SYNTHESIS |
1990 |
- V.N.Mallikardzhuna Rao[Us]
|
RU2021243C1 |
| METHOD OF SEPARATING FLUOROOLEFINS FROM HF BY LIQUID-LIQUID EXTRACTION |
2007 |
|
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| METHOD FOR PRODUCTION OF FLUORINATED HYDROCARBONS |
1997 |
- Mario Dzhozef Nappa
- Vil'Jam Robert Vil'Jams
|
RU2150454C1 |
| CONTINUOUS METHOD OF 1,1-DICHLOROTETRAFLUOROETHANE SYNTHESIS |
1990 |
- Uil'Jam Genri Gumprekht[Us]
- Dzhon Mark Longoria[Us]
- Frank Dzh.Kristof[Us]
|
RU2010789C1 |
| METHOD OF 1,1,1-TRIFLUORODICHLOROETHANE AND 1,1,1,2-TETRAFLUOROCHLOROETHANE SYNTHESIS |
1988 |
- Vil'Jam Genri Gamprekht[Us]
- Leo Ehrnst Mehnzer[Ca]
- Vellijur Nott Mallikardzhuna Rao[Us]
|
RU2007380C1 |
| SATURATED LINEAR POLYFLUOROHYDROCARBONS, METHOD OF THEIR SYNTHESIS (VARIANTS), COMPOSITION FOR SOLID SURFACE CLEANSING |
1991 |
- Karl Dzhordzh Krespan[Us]
- V.N.Mallikarjuna Rao[Us]
|
RU2073664C1 |
